Connecting a hybrid supercapacitor to an electrochemical workstation (ECW) necessitates a few stages and considerations, including the type of supercapacitor, ECW, and experiment to be done. ECWs of various varieties have varying capabilities and interfaces. It is critical to select an ECW that is compatible with the supercapacitor and the experiment. The supercapacitor will have a positive and negative terminal that should be linked to the ECW's positive and negative terminals. The ECW will be able to regulate the voltage across the supercapacitor and measure the current as a result of this. The ECW may need to be set up with appropriate voltage or current ranges or waveforms depending on the sort of experiment being conducted. Depending on the experiment being run and the kind of supercapacitor used, this will change. The experiment can be carried out once the supercapacitor is attached and the ECW is set up. The supercapacitor may be charged and discharged, the current and voltage may be measured, and data may be analysed.