Dear All,
In XRD data, How the addition of organic additive influenced the average size of the crystallites of metal electrodeposition (Electroplating)?
Regards,
Hani
Dear Dr. Hani Khalil Ismail,
I suggest you to have a look at the following, interesting thesis/papers:
-Influenceof Additives on Electrodeposition of Metals from Deep Eutectic Solvents
By Hasan Fisal AL-Esary - Thesis submitted for the degree ofDoctor of Philosophy At the University of Leicester (2017)
Available at: https://www.google.it/url?sa=t&rct=j&q=&esrc=s&source=web&cd=&ved=2ahUKEwio9du7yLvrAhWCi1wKHZKSDsQQFjAJegQIBBAB&url=https%3A%2F%2Fs3-eu-west-1.amazonaws.com%2Fpstorage-leicester-213265548798%2F18465047%2F2017alesaryhfphd.pdf&usg=AOvVaw0YBr3fW9qGN3VLGOEvD4P8
-A Review of Nanostructural Aspects of Metal Electrodeposition
Luisa Peraldo Bicelli, Benedetto Bozzini, Claudio Mele, Lucia D'Urzo
Int. J. Electrochem. Sci., 3, 356 – 408 (2008)
Available at: http://www.electrochemsci.org/papers/vol3/3040356.pdf
-Characterization of Defect Structure in Electrodeposited Nanocrystalline Ni Films
Tamás Kolonits, Péter Jenei, Bence G. Tóth, Zsolt Czigány, Jenő Gubicza, László Péter and Imre Bakonyi
J. Electrochem. Soc.163 (3), D107-D114 (2016)
Available at: https://arxiv.org/ftp/arxiv/papers/1703/1703.05191.pdf
-Glycerol Effect on the Corrosion Resistance and Electrodeposition Conditions in a Zinc Electroplating Process
Michele David de Jesus Almeida, Carlos Alberto Della Rovere, Luiz Rogério Pinho de Andrade Lima, Daniel Veras Ribeiro, Carlos Alberto Caldas de Souza
Mat. Res., 22, 4 (2019)
Available at: https://www.scielo.br/scielo.php?pid=S1516-14392019000400219&script=sci_arttext
Best regards, Pierluigi Traverso.
Dear Dr. Hani Khalil Ismail,
I suggest you to have a look at the following, interesting thesis/papers:
-Influenceof Additives on Electrodeposition of Metals from Deep Eutectic Solvents
By Hasan Fisal AL-Esary - Thesis submitted for the degree ofDoctor of Philosophy At the University of Leicester (2017)
Available at: https://www.google.it/url?sa=t&rct=j&q=&esrc=s&source=web&cd=&ved=2ahUKEwio9du7yLvrAhWCi1wKHZKSDsQQFjAJegQIBBAB&url=https%3A%2F%2Fs3-eu-west-1.amazonaws.com%2Fpstorage-leicester-213265548798%2F18465047%2F2017alesaryhfphd.pdf&usg=AOvVaw0YBr3fW9qGN3VLGOEvD4P8
-A Review of Nanostructural Aspects of Metal Electrodeposition
Luisa Peraldo Bicelli, Benedetto Bozzini, Claudio Mele, Lucia D'Urzo
Int. J. Electrochem. Sci., 3, 356 – 408 (2008)
Available at: http://www.electrochemsci.org/papers/vol3/3040356.pdf
-Characterization of Defect Structure in Electrodeposited Nanocrystalline Ni Films
Tamás Kolonits, Péter Jenei, Bence G. Tóth, Zsolt Czigány, Jenő Gubicza, László Péter and Imre Bakonyi
J. Electrochem. Soc.163 (3), D107-D114 (2016)
Available at: https://arxiv.org/ftp/arxiv/papers/1703/1703.05191.pdf
-Glycerol Effect on the Corrosion Resistance and Electrodeposition Conditions in a Zinc Electroplating Process
Michele David de Jesus Almeida, Carlos Alberto Della Rovere, Luiz Rogério Pinho de Andrade Lima, Daniel Veras Ribeiro, Carlos Alberto Caldas de Souza
Mat. Res., 22, 4 (2019)
Available at: https://www.scielo.br/scielo.php?pid=S1516-14392019000400219&script=sci_arttext
Best regards, Pierluigi Traverso.
Dear all, the following RG document discusses this subject. Better answers may be added if the whole system in mentionned. My Regards
https://www.researchgate.net/publication/240368692_The_influence_of_organic_additives_on_the_electrodeposition_of_iron-group_metals_and_binary_alloy_from_sulfate_electrolyte
Addition of organic additives having higher number of phenyl or unsaturated groups tend to enhance the crystallization process.
Hi
The addition of organic additive does influence the average size of the crystallites of metal electroplating. This because the additive can be either inhibiting,, retarding, or catalyzing the nucleation and growth of the crystallites of metal electroplating.
see the following link for more information
Article Additives for morphology control in high-efficiency organic ...
Dear all, in the physical-chemistry of materials field, there are two types of chemicals regarding the control of order/disorder of a given structure formation from solution/melting, these are structure: structure forming and structure breaking chemicals. The first type is better known as nucleating agents which promote and control the crystal growth. The best exemple of the second type is urea with respect to water. So, it depends on the type of the organic compound nature, either crystalline or amorphous structures are produced. My Regards
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