If you mean transferring Powder X-Ray Diffraction (PXRD) to Crystal Structure, you need to do Structure Solution from Powder X-Ray Data (SDPD). It is realy time consuming and proffessional process. Then you need to ask an expert to do it, if they find it worthwhile.
Saba Alasalli - you have to grow a crystal. There are many techniques - main ones possibly using a flux or floating zone in an image furnace... Try Wikipedia.