21 September 2019 0 3K Report

I am trying to prepare the nickel sulphide (NiS )from mixing of nickel nitrate Ni(NO3)2 sodium sulphide in equal amounts and then pass H2S gas and few ml SDS also mixed in solution .The solution can be stirred by using magnetic stirrer at room temprature for 20 to 30 minutes. But black ppt of NiS can not be obtained.

plz any one guide me.

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