I want simple qualitative methods to evaluate the evaporation of volatile solvents from a solution.
For example, if I have DCM in a solution and I am evaporating it, how can I know that after one hour if it is completely evaporated from solution?
Simple way weighting or observing the constant weight on the balance. Or using the headspace technique e.g. SPME and determine by GC
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06 July 2014 2,390 1 View
I prepared microparticles but the problem is that the encapsulation efficiency very low. My polymer is Ethylcelluose and my compound is soluble in both the aqueous phase and organic phase. I...
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I am looking for the best polymer which also has a high cross-linking matrix.
09 October 2013 4,106 4 View
Simple method to predict the degradation of a compound during solubility study
09 October 2013 7,724 28 View
Any suggestion to do solubility study for a compound that I have a very small amount of it and I want to test its solubility in different solvents.
09 October 2013 7,548 6 View
I am making polymer composite by solvent mixing method. When I am trying to add filler solution in polymer solution it quickly get solidified. How to make them then uinform? It doesn't give time...
03 March 2021 7,540 4 View
dear community, my model is based feature extraction from non stationary signals using discrete Wavelet Transform and then using statistical features then machine learning classifiers in order to...
03 March 2021 6,994 5 View
I am try to make the Paal Knorr reaction between 2.5 hexnedione and 6-amino hexanoic acid, my problem is type of solvent to use, because 6-hexaminohexanoic acid is soluble in water but I am not...
02 March 2021 4,443 2 View
I want to polymerize TEOS on a surface. I know that NH4OH is a preferred catalyst and an alcoholic solvent should be used .But I can not find certain amounts of each material to use. Does any one...
02 March 2021 1,404 6 View
I need a procedure to extract the ciprofloxacin hydrochloride from aqueous solution by using dichloromethane in detail,. I thank you very much.
01 March 2021 4,306 1 View
I am currently doing my third year design project. I have been assigned to design a glycerol recovery column in vinyl acetate monomer production. The process unit before the recovery column is an...
01 March 2021 9,525 4 View
The resultant solid was partitioned three times with 250 ml of petroleum ether (40-60/c) to remove any fatty material and evaporated to dryness.
28 February 2021 9,464 2 View
Favourable conditions of base pressure, rate of deposition. Also, by which characterisation technique to be used to verify the thickness of the deposited film.
28 February 2021 3,640 3 View
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The reaction of APTES with salicylaldehyde in ethanol leads to the formation of imine compound yellow solid which is mention in literature, but I am not getting yellow solid I don't know why? when...
28 February 2021 2,955 2 View