I have made mathacrylated gelatin using the protocol in the attached paper. The powder seems to look fine and is easily dissolved in PBS. I tried to make a 5% w/v prepolymer solution containing 0.5% w/v irgacure 2959. After exposing to UV for 30s, I don't observe any gelation. I increased the irgacure to 1% and after 3 minutes of exposure a pale yellow gel was formed, but I'm assuming this time is too long and the formed gel is not what I'm looking for. Appreciate any ideas on this issue. Thank you