Hello! I am a PhD student in Chemistry and I am traying to synthetize gamma-cyclodextrin MOFs with KOH following different methodologies that I have found in papers (vapor diffusion method, microwave method,...). In order to characterize the structures and confirm that I have obtained these MOFs, I did measurements by PXRD, but the difractograms that I get it are not good enough (wide peaks like a mountain), it seems that the structure is amorphous.
Does someone have any idea that how can I work with these kind of MOFs?
Thank you very much in advance!
Best regards,
Jorge
not used KOH but use NaOH???????????????? you can obtained you XRD?????
Thank's
Thank you very much for your answer Abdelkader Rahmouni. I always read the synthesis of these kind of MOFs with KOH, is the NaOH better? Do you have any reference?
Thank you in advance,
Jorge
1-you can see this thesis of my laboratory?????
2-you can see my paper
my best regard's
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