Aoa I have performed Dsc. the picture is attached. kindly help me explain the machine gave the detail under glass transition.. crystallinity id 1069.69 % what does it means ?
You need to remove the isothermic parts and normalize to sample size. It should then be possible to get a better view on possible 1st or 2nd order transitions.
@Günther W. H. Höhne sir the dsc i operated it was adjusted to these settings heat flow versus time, and tried to find out the glass transition and these were the results machine showed !