I have prepared same mix metal hydroxide adsorbent by sol gel method, and calcined it to 300 deg C, interested to understood the exact bonding between different metals oxides/hydroxides. if someone did such kind of exercise kindly direct me about how to get predict that.
If I got your question, you are trying to prepare mixed metal oxides/hydroxides using sol gel method, and you are asking about the common bonds in your material after calcination at 300oC.
More information about your sample is required to get specific answer. However, generally speaking, the type of bonds in the material depends mainly on the phase composition as well as the chemical composition. To have an idea about the thermal behavior of your dried gel during the calcination, DTA and TGA are required. Also, XRD is necessary to know the phase composition. FTIR is also important to such study.
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