My experiment involves Na-ion intercalation in carbonate based electrolyte using a 3-electrode cell with a Ag/AgNO3 reference electrode.
1) If my electrolyte is 1M NaClO4 in PC/DEC, do I use that same solvent with 0.001M AgNO3 and 0.1 M TBAP in my reference cell?
2) Does the selection of supporting electrolyte (0.1M TBAP) important? Could I just use my 1M NaClO4 from my original electrolyte? This would minimize the liquid junction potential, right?
Dear Sir
I think the links below will benefit you in your search
http://www.rsc.org/suppdata/c6/ta/c6ta00313c/c6ta00313c1.pdf
https://gupea.ub.gu.se/bitstream/2077/34583/1/gupea_2077_34583_1.pdf
https://etd.ohiolink.edu/rws_etd/document/get/case1270148716/inline
https://www.als-japan.com/1389.html
https://link.springer.com/content/pdf/10.1007%2F978-3-642-36188-3.pdf
Best Regards
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