I synthesis silver nanoparticle by one step method (good dispersed and don't settle from medium) and I am't able to separate it from medium. I get XRD pattern and how check it? is it comparable with XRD pattern from silver solid?
Dear Hamid Mosaddeghi :
This issue was discussed.
https://www.researchgate.net/post/Can_any_one_explain_the_broadening_of_XRD_peaks_of_nanoparticles_compared_to_those_of_the_corresponding_raw_materials
https://www.researchgate.net/post/How_are_silver_nanoparticles_dried_so_as_to_measure_their_particle_size_in_X_Ray_diffraction
https://www.researchgate.net/post/I_have_synthesized_Cobalt_Oxide_nanoparticles_but_the_powder_XRD_pattern_is_giving_no_peaks_What_could_be_the_possible_reasons
Best regards
It would be meaningless to obtain conventional XRD pattern for nanoparticles dispersed in a fluid. What you need is SAXS. XRD difractograms and SAXS results are not necessarily that much related. Apparently, SAXS is available in Iran. Last time I checked, Iran polymer and petrochemical institute has one that performs liquid state characterizations.
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