because i try to refine BCSA clinker with Rietveld refiment and i cant match some peaks. especially 2theta :32.3, 37.5, 53.9, 64.26 values peaks cant refine.
secondly; i can't find any proper phases for MgO and i think these peaks which can't fit, belong to some Mg included structure.
Ian J Slipper
Please post your raw data, preferably as .xy or .raw file and show what qualitative assessment you have done so far. Starting a quantitative Rietveld analysis with incorrect or incomplete phases is the path to disaster.
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Ian J Slipper
The peaks you cannot identify are all from lime (CaO).
Periclase (MgO) is there at 42.92 2-th, way down in the background.
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