07 August 2021 3 3K Report

I want to determine concentration of Urea in a given aqueous sample and following micro Kjeldahl process initiating the digestion process with H2SO4 + other catalyst, total vol is 100ml. During digestion this volume is getting evaporated within10 mins.. Can someone guide me if

1. My process is right?

2. what should be the digestion time & temp?

3. what should be the approximate volume which should to next process of NaOH distillation. Thank you for assisting.

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