Selecting a good potential windows in CV

01 January 1970 0 8K Report

What is the best suitable way to select potential windows in CV. Currently, I am doing cyclic voltametry for bulk MoS2, WS2 and MoSe2 for homo and lumo energy level calculation. I am using 0.5 M KCl as an electrolyte and Ag/AgCl reference electrode. What will be the best potential window for this reaction and how to determine that?

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