hello

during synthesis de titanium dioxide via Sol gel using this molar ratios

TTIP: EtOH: water: HCl  1: 4: 10: 0.5 respectively for this i prepared solution 1 that content TTIP dissolved in ethaol thes this solution is added dropwise under stirring to the second solution (water+ HCl) i obtained trouble solution and this later is kept for 24 hours to form gel

the pH of second solution( water+ HCl) is -0.78

the problem is: there is no gel formed but the sol is turned transparent?

how i do to increase time of gelation? 

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