I get high intensity peak 2theta at 30 degree for graphene oxide.what it means ? & How to eliminate it?

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Mohammed Hussein j. H. Al'Atia

Dear Gauri Patil

The high intensity peak 2 theta at 30o for graphene oxide indicate the unsuccessful oxidation process for the residual raw graphite. Once the graphite is totally oxidized , this peak eliminated and no longer be observed. Best regards ....

Gauri Patil

Thank you sir.

One more query, how to do complete oxidation of that incomplete oxidised graphene?

Thank you for your feedback. I enclose set of published papers contains a helpful guide knowledge related your last query.Hope the task is easy for you. Wishing you progress and success with my best regards....

https://pubs.acs.org/doi/10.1021/acsomega.2c01963#:~:text=independent%20chemical%20reaction.-,Mn2O7%2C%20the%20main%20oxidant%2C%20is%20heated%20to,H2SO4–GIC.

https://www.sciencedirect.com/science/article/abs/pii/S0008622320304462

https://www.sciencedirect.com/science/article/abs/pii/S2352492823012680

Article Studies of Reduced Graphene Oxide and Graphite Oxide in the ...

Article Structural Evolution of Hydrothermally Derived Reduced Graphene Oxide