is there any problem with my method, if someone can refer me to correct method ?
can someone guide me with variables to get perfect results for rubbers. although i am trying variation, yet unable to see Ea in rsulted data through TRIOS software
I am not sure if this will help you, but when I calculate the activation energy and pre-exponential factor I use the Flynn-Wall method. Here's the reference:
J.H. Flynn, L.A. Wall, J. Polym. Sci. C. Polym. Lett. 4 (1966) 323e328
Heating rate was 20, 50 & 100, with amplitude of 4-5 and was varying time b/w 100-200 s. i will try now with heating rate of 2, lets see if i get something. thank you so much, maybe i'll ask more questions :)