I already tried to recrystallize it using ethanol and there is no sign of crystals or formation of solid. The solid crude product is insoluble in DCM, ethyl acetate, chloroform even at higher temp. But the solid is soluble in DMSO.
Talaat I. El-Emary
Dear Benhur Medija
Did u try dissolve the product in DMF?. Also, how many spots in tlc test?
Good luck
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Vidyadhar Gawandi
If your crude product is insoluble in water at room tempr then try to crystalise it in 50-75% water in DMF or DMSO. Good Luck
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Jamatsing D Rajput
Dear,
Used mixed solvent system like ethyl acetate + Ethanol or Methanol
as per solubility of your compound
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