We are studying on PEMFC electrocatalysts via magnetron sputter systems on carbon paper substrates. By this way we can perform CV and RDE experiments without using ionomer dispersion.

Right now i have to decide on the preparation method of MEA.

-I am worried about if micropippet drop or spray bottle is the best ionomer coated method? (I don't have any other option, maybe paint brush)

-What should be starting value for the ionomer/catalyst mass ratio?

-Can temperature of hot press be a reason of agglomeration of particles (above T=100C)?

-Thickness of the catalytic thin film is blow 50 nm.

Thank you.

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