I am preparing chitosan film by casting chitosan solution into petri dish and let it air dry. I am using NaOH to peel off the dried film but it breaks the film. I have used different molar strengths of NaOH 0.01 to 0.1 M. But film breaks down.
Peeling off chitosan film from a petri dish can be challenging, and the use of NaOH to aid in the peeling process may not always be successful, as you have experienced. Here are some alternative methods that you can try:
Use a non-stick surface: Instead of using a petri dish, you can try casting the chitosan solution onto a non-stick surface such as a Teflon sheet or a silicone mat. This will allow the film to be easily peeled off without the need for NaOH.
Use a different alkaline solution: Instead of using NaOH, you can try using other alkaline solutions such as potassium hydroxide (KOH) or ammonium hydroxide (NH4OH) to aid in the peeling process. These solutions may be less harsh on the chitosan film and less likely to cause breakage.
Adjust the drying conditions: The drying conditions of the chitosan film can affect its adhesion to the petri dish. To improve the adhesion of the film to the dish, you can try increasing the drying time or using a lower temperature for the drying process. This can help the film to adhere better to the dish, making it easier to peel off.
Use a peel test: If the film still breaks when peeled off, you can try performing a peel test to evaluate the strength of the film. This involves using a machine to peel the film off the surface and measure the force required to peel it off. This can help you to optimize the film preparation conditions to achieve a film that is both strong and easy to peel off.
Overall, there are several methods that you can try to peel off chitosan film without using NaOH, including using a non-stick surface, using a different alkaline solution, adjusting the drying conditions, and performing a peel test.