I would like to design a home-made set up to examine gas adsorption performance of solids toward certain gases via a volumetric approach. To do this, the volume of loading and sample cells must be estimated. According to literature, the larger in volume the sample cell is, the higher the amount of loaded adsorbent is , but I do not have any idea about the proportion existing between these two parameters. Despite my extensive researches, I did not come up with much information, so could anyone please give me some advice on the effects of cell volume and the weight of adsorbent? It should be declared that loading of lower amount of adsorbent is preferred.

thank you in advance