I have a 750 ml reactor and working volume is 300 ml. my working temperature is 350 C. By using ideal gas law i found at the pressure to be around 2 bar. But  I need final pressure build up @ 350 C to be around 25Mpa in order to keep my solvent in liquid phase. So, how should i calculate the initial  head space pressure required. I'm planing to use N2 gas for pressure build up

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