What is the problem in attached file?

I have done ORR LSV (attached file) at different RPM (400-2000) in 0.1M KOH electrolyte (PH=13) using RDE. My teacher said that it is wrong due to limiting current density. Kindly give me your...

08 September 2019 1,662 2 View

How to do Particle Size Distribution of very small particles?

I used Image j but I didn't get correct result, is there another way to calculate particle size?

05 June 2019 8,862 3 View

What is the correct way of conversion of ppm to ppb?

Please suggest me a correct method of dilution of solutions to convert ppm to ppb. Let suppose I have 0.05 mg/ml solution, it has 50 ppm and I want to convert into different ppb solutions like 50,...

04 May 2019 9,307 1 View

How I can match simulated and own XRD pattern in Origin?

Hi, I have used American Mineralogist crystal database and downloaded .cif files and then used VESTA software to simulate XRD pattern and also have jcpdf number, I want to match with my own XRD...

04 May 2019 1,468 4 View

How can a beginner learn the analysis of X-ray photoelectron spectroscopy (XPS) by himself?

Is there any literature or trilaterals?

04 May 2019 3,309 6 View

Can anyone provide me JCPDS files?

Hi, everyone, I needed JCPDS files of Pt, Cu, PtCu & Cu3Pt, if anyone have then please share with me, I will be highly thankful. File numbers are as follows: PtCu = JCPDS 48-1549 Pt = JCPDS...

04 May 2019 1,856 4 View

What does it mean pass/fail in BET result?

I did BET for my catalyst (PtCu Nano particles) when I got result, I saw this error (given in attached figure), as BET Surface area is too low, what does "fail'' mean? is it incomplete analysis or...

03 April 2019 7,043 10 View

How can a beginner learn the analysis of XRD Powder method by himself?

Is there any literature or trilaterals?

01 February 2019 4,976 12 View

What is the standard electrode potential of Hg/HgO ?

01 February 2019 4,924 3 View

How to convert a potential collected with reference to Hg/HgO to Reversible Hydrogen Electrode?

I have collected a LSV data by taking Hg/HgO as the reference electrode. But I want to convert this one to RHE. Please suggest me the required conversion equation. 0.1M KOH was taken as the...

01 February 2019 6,730 4 View

flexibility of polymers chain

effect of double bond on the flexibility of polymers

07 April 2021 0 0 View

Formulation of polymer color flakes

I am writing to request some information for making polymer color flakes. I would appreciate the help.

17 March 2021 0 0 View

Polymer composites suddenly solidifies?

I am making polymer composite by solvent mixing method. When I am trying to add filler solution in polymer solution it quickly get solidified. How to make them then uinform? It doesn't give time...

03 March 2021 7,540 4 View

What techniques can I use to determine the miscibility of polymer blends?

The term miscibility refers to the single-phase state in thermodynamics. I do not mean the compatibility of different components. To determine the miscibility I know several techniques such as...

03 March 2021 4,107 4 View

How the parameters (such as Mw, Chemical bonds, polymer bland and so on) affect the mechanic property of polymer (such as storage, loss modulus) ?

Anyone can recommend any books on such topics? Thanks in advance.

02 March 2021 8,457 2 View

How do I determine the degree of polymerization of PEG 400 based on NMR integration?

Hello, I am working on the photocatalytic degradation of PEG 400. I would like to know if it's possible to determine the degree on polymerization based on NMR integration, or by the MW of the...

02 March 2021 6,186 3 View

How to polymerize TEOS?

I want to polymerize TEOS on a surface. I know that NH4OH is a preferred catalyst and an alcoholic solvent should be used .But I can not find certain amounts of each material to use. Does any one...

02 March 2021 1,404 6 View

Can polymer concentrations be calculated based on the number average molecular weight?

Hello, I spin-cast two different polymers onto wafers and measure their height as a function of initial concentration. For polymer A, I have the weight-average molecular weight (Mw) as well as...

28 February 2021 7,882 2 View

What is the density for pva electrospining?

I'm Juan Carlos, a high school student who is working with electropinning, I made an electropinning machine with a 21g needle and a 30kv high voltage source and the distance between my needle is...

28 February 2021 298 3 View

POlymer+DMSO solution and moisture??

What could be the reason of moisture at the sides of Vial when I am preparing my polmyer+DMSO solution for membrane fabrication? What etiquettes I am possibly missing here?

28 February 2021 6,516 5 View