Hi there,

We usually purge our electrolyte to remove all the dissolved Oxygen, before running electrochemical tests. Most researchers use Ar or N. Also most researchers purge for around 0.5 hours for about 100ml solution. I have also read a systematic study where they have proved that 0.5 hrs should be ideal  and would lead o about 0.5ppm (don't remember the exact value!). But I have never seen anyone talking about the flow rate of purging. While large flow rate quickens the process (large bubbling). Or is low flow rate more helpful in saving Ar/N?

I am curious to know about this and electrochemists experience!

regards

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