I fabricated RuI3 with CVT method, but I am not sure that this material is RuI3 or other Ru compounds. I checked the reference that one paper (published in 1968) had analysed the structure of RuI3 by XRD but they didn`t show the diagram. Does anyone know where I could get the XRD diagram of RuI3? Thank you very much!
Professor Anan F Rawle, Thank you for your answer. RuI3 studied in this dissertation is with a amorphous form, but in my case , the RuI3 exists in a crystal morphology. A dissertation of H. K. Breitbach may be contain the XRD information of RuI3 according the paper I read(in the attachment) , but the dissertation is old, published in 1967, I can´t download it in my institute. Thanks again for your help.
Rong Sun OK, understood. You could try writing directly (on a postcard? As we used to do in the old days.....) to the Institute concerned (probably the library). They may be able to send you an on-line link or generate a copy (probably you'd have to pay for the latter). More information in the attached but again the information for RuI3 is limited (page 59 in the thesis).
Structural Investigations of β -RuCl3, RuBF3 and RuI3h. g. von schnering, k. brodersen, f. moers, h. k. breitbach and g. thiele, J. Less-Common Metals, 1966, 11, (4), 288–289The three compounds are of the TiI3 structural type with hexagonal crystals and the following lattice parameters: β-RuCl3, a = 6.126, c = 5.653Å, c/a = 0.923; RuBr3, a = 12.924, c = 5.860 Å, c/a = 0.453; RuI3, a = 6.982, c = 6.231, c/a = 0.892.
I'm sure you've seen the attached too. It seems these authors have great experience in the area and an email or letter to one of them could prove useful.
You can find more information from Jade and crystal
Crystallography Open Database about crystal.
Crystallography Open Database provide online CIF FILE (Download) CIF provides all information such as, angle, distance, site etc, and use Diamond OR MUR CRY to DRAW THE Structure.
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