Currently, I am planning to synthesis of Fe nano particles with aid of an Argon gas to reduce further oxidation during the process. So, I am in need of clear protocol for further proceedings.
I guess that via co precipitation method, after you mix the reactant solutions e.g., ferric nitrate, first use a balloon filled with Ar gas and purge into your sealed beaker (covered with baloon) for 10 to 15 minutes to completely remove oxygen. After that you can add reducing agent, while the balloon is still attached with the beaker. You can use a 2-neck flask for this purpose.
Thanks Mr. Arunkumar Rengaraj and Mr. Muhammed for ur kind reply...But i am opted to work via co-precipitation method. Please send me the reference article for co precipitation method (argon gas environment)...
Thanks Mr. Arunkumar Rengaraj and Mr. Muhammed for ur kind reply...But i am opted to work via co-precipitation method. Please send me the reference article for co precipitation method (argon gas environment)...