Just wondering if anybody has done thermogravimetric analysis on pure hemi and mono carboaluminate phases? I am looking for the mass loss of chemically bound water. Based on the references I have it appears that mono carboaluminate has multiple mass loss endothermic peaks, one below 200 deg, two between 200 and ~320 deg. Another reference shows one upto 200 and the second mass loss goes upto ~350. These are the only two references I have for mono-carboaluminate but I don't have any for hemi-carboaluminate. I have attached one reference in pdf and the other in a research paper:

Iron in carbonate containing AFm phases by B.Z. Dilnesa et al. published in cement and concrete research (2011)

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