I want to ask experimental setup of synthesis of covalent organic frameworks(COF).

In some literature they put all component in "pyrex tube" and apply freeze pump thaw cycle and heated upto certain temperature(120oC).

my questions are

1. what is the pyrex tube exactly and how to cap tightly

2. how to heat pyrex tube?

oven ? silicon oil with hot plate?

3. do we need stirring with magnetic bar? or just keep stayed?

if you have a experience of COF synthesis please give me the answers.

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