Ideally this liquid would evaporate during processing stage (190 C). Many thanks!
How about DMSO (bp 189 C) or water (bp 100C)?
Unfortunately, Amino-POSS seems unstable in water (http://pubs.acs.org/doi/abs/10.1021/acs.jpcb.5b01955)
By the way, are you talking about amino-POSS with 8 amine functions per molecule?
Or only one amine funtion and seven alkyl functions like this one : http://www.sigmaaldrich.com/catalog/product/aldrich/560294?lang=fr®ion=FR
What solvent did you try already?
Best regards
Octa amino-POSS is stable onyly in diluted methanol solution.
For more see:
https://www.researchgate.net/publication/265096300_High-Yield_Synthesis_of_Amido-Functionalized_Polyoctahedral_Oligomeric_Silsesquioxanes_by_Using_Acyl_Chlorides
Article High-Yield Synthesis of Amido-Functionalized Polyoctahedral ...
Pupil Core for simultanious recording of a child and a mum and is willing to share experiences?
07 July 2024 9,066 0 View
Hello, what THP-1 differential markers do you use in the Western-blot method? I am looking for proteins that are characteristic of M0, M1 and M2. Do you have something proven and reliable? Greetings
24 June 2024 9,025 0 View
I was recently performing a great deal of qPCRs on adipose tissue derived RNA. I had experimental samples from sick, and control samples from healthy individuals. I used the same chemistry for all...
04 June 2024 6,924 0 View
For several years now, the procedure of granting a vote of confidence to the municipal executive by the legislative has been in force in Poland. It takes place annually and is not related to the...
16 February 2024 4,769 2 View
I completed the experiment for one of our colaborators (I measured inhibition of an enzyme by 3 compounds). Unfortunatelly compounds were not active in the range of dilutions that I had used (up...
06 February 2024 3,542 2 View
Climate change is one of the most serious challenges humanity has ever faced. To address the problem UN Framework Climate Change Convention was established Climate change education has been a...
07 September 2023 2,621 2 View
I have the lite version of ZEN ZEISS 3.7 software and I can't use the "Image Analysis" option because it is only available in the blue version. Is there another way to count the number of...
26 July 2023 7,426 1 View
Dear Colleagues, which software is in your experience most suitable for analysing semi-structured interviews? Can you give examples of articles where such data were analysed and results...
14 December 2022 9,735 4 View
Hello RG, I have results from Sanger sequencing for validation of multiple variants I have found in my patients cohort, can you please instruct me if there is some sort of open source program...
21 August 2022 1,286 0 View
Dear fellow Researchers, I have a question - can anybody explain, show literature sources or in any other way guide our team in the complex topic of mechanisms of uptake of organic contaminants...
08 August 2022 4,974 2 View
I'm currently working on calculating the collision cross section (CCS) for various ions, and I'm facing challenges when dealing with sodiated and multiply charged ions. Most of the resources I’ve...
08 August 2024 8,329 0 View
I conducted an adsorption experiment of arsenic on soil in the presence of different doses of silicon as competing ions to see the effect of silicon on arsenic adsorption and desorption. I took 5...
03 August 2024 6,500 3 View
I am currently working on a project involving liposomes and need to determine the maximum volume of siRNA that can be added to a 2.5 mL liposome solution with a total lipid concentration of 10...
30 July 2024 6,420 1 View
Dear Siesta Users, I installed Siesta 5.0.1 and I want to use Grimme's D3 correction. According to the 5.0.1 manual, I could use a few parameters to include the D3 correction in the...
27 July 2024 5,748 0 View
It has been long known that EDC carbodiimide and NHS easter's half life agains hydrolysis are highly related to pH. However, very surprisingly, not yet found a paper giving a table/chart of their...
25 July 2024 8,738 0 View
I run mechanochemical reactions that involves the use of a large amount of catalyst (1:1 molar ratio to the reactant). When I try to understand the effect of amount of catalyst on the reaction, I...
23 July 2024 9,938 1 View
Hi, I am a PhD student working at Jagiellonian University, Faculty of Chemistry. My work is related to the development of new analytical methods for the quantification of short-chain fatty acids...
22 July 2024 5,492 6 View
Dear Researchers, My question is associated with the "MDCI" method in Orca. Please let me clarify my question using a simple example: Suppose we are going to perform CBS extrapolation using "!...
21 July 2024 1,632 0 View
I do not know much about FTIR! The material Benzethonium Chloride USP was compared to a reference standard in regards to FTIR, as per the USP testing: Identification B. Infrared absorption (FTIR),...
16 July 2024 6,918 7 View
Dear all, I have a question regarding ways to separate ammonium nitrate and phosphorus pentoxide?
12 July 2024 3,164 2 View