could any one suggest me ??

11 September 2018 0 3K Report

To make crystal for polymeric form of Fe complexes? Initially it is soluble in DCM after tried it or powder form, not even dissolve in DCM or ACN or Ethylacetate or Any non- polar solvent. But, it is quite soluble in DMSO only.

when i dissolve the powder form of Fe complex in DCM for making crystal (through layering or slow diffusion), Initially it's dissolve after certain time it is start to settle down.

Particularly, it is not stable in air, moisture and light. Either reaction or workup i always covered with foil paper (Ar atmosphere)

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