I have tried sol-gel method using the PEG 2000 and 20000 and the final result was yellow agglomerated granules on the surface without any connection to the substrate!

I have some limitations such as using Just Titanium IV butoxide or Titanium iso propoxide as the titanium precursor for the diposition.

could you suggest the modification for the method or a simple new method (something like wash-coat) solving the problem?

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