Can one trust rapid thermal crystallization of metal complexes for X-ray single crystal measurement?

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Niyazi A. S. Al-Areqi

The method you used in your published work " Synthesis, spectral, thermal, X-ray single crystal of new RuCl2(dppb)diamine complexes and their application in hydrogenation of Cinnamic aldehyde" , seems efficient for such metal complexes you prepared. However, you can also find alternative methods in this site

http://www.southampton.ac.uk/xray/links/crystalgrowth/grow1.htm

Ismail Warad

Yes Dr. Al-Areqi

thank you for the fruitful link

but some time you collected v. nice, due to unknown reason it did not diffract.