How can we make an ORTEP view of Schiff base complexes using powder XRD?

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Melanie Pilkington

You will need to do a Rietveld refinement of your powder data and output a .res file that can be read into ORTEP.

Erik Rakovský

... and it isn't by any means routine :D

Preferably, you need not only XRD but preferably also neutron powder diffractogram, both with a suitable angular resolution. For basic introduction you can try Jana2006 software (http://jana.fzu.cz) with some examples (Jana Cookbook, http://jana.fzu.cz/workshops/cookbook.zip).