I have to separate some enantiomers but i have no ideas about what i have to do! So if you know some good books in this field please tell me! Thanks so much!
Dear Tuan,
The following are the required books:
1-Enantiomer Separation -Fundamentals and Practical Methods
Editors: Toda, Fumio (Ed.)
ISBN 978-1-4020-2337-8
http://www.springer.com/br/book/9781402023361
About the book:
In spite of important advances in asymmetric synthesis, chiral compounds cannot all be obtained in a pure state by asymmetric synthesis. As a result, enantiomer separation remains an important technique for obtaining optically active materials. Although asymmetric synthesis is a once-only procedure, an enantiomer separation process can be repeated until the optically pure sample is obtained. This book discusses several new enantiomer separation methods using modern techniques developed by experts in the field. These methods consist mainly of the following three types: 1) Enantiomer separation by inclusion complexation with a chiral host compound 2) Enantiomer separation using biological methods 3) Enantiomer separation by HPLC chromatography using a column containing a chiral stationary phase. Separation of a racemic compound has been called “optical resolution” or simply “resolution”. Nowadays, the descriptions “enantiomer resolution” or “enantiomer separation” are also commonly used. Accordingly, “Enantiomer Separation” is used in the title of this book. The editor and all chapter contributors hope that this book is helpful for scientists and engineers working in this field.
2- Separation of Enantiomers: Synthetic Methods
Matthew H. Todd (Editor)
ISBN: 978-3-527-33045-4
312 pages
June 2014
Home / Chemistry / General Chemistry
Separation of Enantiomers: Synthetic Methods
Matthew H. Todd (Editor)
ISBN: 978-3-527-33045-4
312 pages
June 2014
Read an Excerpt
Description
In one handy volume this handbook summarizes the most common synthetic methods for the separation of racemic mixtures, allowing an easy comparison of the different strategies described in the literature.
Alongside classical methods, the authors also consider kinetic resolutions, dynamic kinetic resolutions, divergent reactions of a racemic mixture, and a number of "neglected" cases not covered elsewhere, such as the use of circularly polarized light, polymerizations, "ripening" processes, dynamic combinatorial chemistry, and several thermodynamic processes.
The result is a thorough introduction to the field plus a long-needed, up-to-date overview of the chemical, biological, and physical methods and their applications. Newcomers to the field, students as well as experienced synthetic chemists will benefit from the highly didactic presentation: Every method is presented in detail, from relatively simple separation problems to advanced complex resolution methods.
Table of Contents
INTRODUCTION: A SURVEY OF HOW AND WHY TO SEPARATE ENANTIOMERS
Classical Methods
Kinetic Resolution ('KR')
Dynamic Kinetic Resolution ('DKR')
Divergent Reactions of a Racemic Mixture ('DRRM')
Other Methods
STOICHIOMETRIC KINETIC RESOLUTION REACTIONS
Introduction
Kinetic Treatment
http://eu.wiley.com/WileyCDA/WileyTitle/productCd-3527330453.html
3-Chiral Separations: Methods and Protocols
https://books.google.ps/books?isbn=1592596487
Gerald Gübitz, Martin G. Schmid - 2004 - Science
Conventional methods for enantiomer separation on a preparative scale are fractionated ... It is not the aim of this book to give a comprehensive overview of all
https://books.google.ps/books?id=dmEyRNY-5owC&pg=PR5&lpg=PR5&dq=books+about+techniques+for+separating+enantiomers&source=bl&ots=Ly3ZabHYVT&sig=gQvmG0sfnSILRrIh5OtDCv2B5as&hl=en&sa=X&ved=0ahUKEwivm7ni1IHKAhWLvnIKHUGoDGgQ6AEILzAE#v=onepage&q=books%20about%20techniques%20for%20separating%20enantiomers&f=false
Hoping this will be helpful,
Rafik
Dear Tuan,
The following are the required books:
1-Enantiomer Separation -Fundamentals and Practical Methods
Editors: Toda, Fumio (Ed.)
ISBN 978-1-4020-2337-8
http://www.springer.com/br/book/9781402023361
About the book:
In spite of important advances in asymmetric synthesis, chiral compounds cannot all be obtained in a pure state by asymmetric synthesis. As a result, enantiomer separation remains an important technique for obtaining optically active materials. Although asymmetric synthesis is a once-only procedure, an enantiomer separation process can be repeated until the optically pure sample is obtained. This book discusses several new enantiomer separation methods using modern techniques developed by experts in the field. These methods consist mainly of the following three types: 1) Enantiomer separation by inclusion complexation with a chiral host compound 2) Enantiomer separation using biological methods 3) Enantiomer separation by HPLC chromatography using a column containing a chiral stationary phase. Separation of a racemic compound has been called “optical resolution” or simply “resolution”. Nowadays, the descriptions “enantiomer resolution” or “enantiomer separation” are also commonly used. Accordingly, “Enantiomer Separation” is used in the title of this book. The editor and all chapter contributors hope that this book is helpful for scientists and engineers working in this field.
2- Separation of Enantiomers: Synthetic Methods
Matthew H. Todd (Editor)
ISBN: 978-3-527-33045-4
312 pages
June 2014
Home / Chemistry / General Chemistry
Separation of Enantiomers: Synthetic Methods
Matthew H. Todd (Editor)
ISBN: 978-3-527-33045-4
312 pages
June 2014
Read an Excerpt
Description
In one handy volume this handbook summarizes the most common synthetic methods for the separation of racemic mixtures, allowing an easy comparison of the different strategies described in the literature.
Alongside classical methods, the authors also consider kinetic resolutions, dynamic kinetic resolutions, divergent reactions of a racemic mixture, and a number of "neglected" cases not covered elsewhere, such as the use of circularly polarized light, polymerizations, "ripening" processes, dynamic combinatorial chemistry, and several thermodynamic processes.
The result is a thorough introduction to the field plus a long-needed, up-to-date overview of the chemical, biological, and physical methods and their applications. Newcomers to the field, students as well as experienced synthetic chemists will benefit from the highly didactic presentation: Every method is presented in detail, from relatively simple separation problems to advanced complex resolution methods.
Table of Contents
INTRODUCTION: A SURVEY OF HOW AND WHY TO SEPARATE ENANTIOMERS
Classical Methods
Kinetic Resolution ('KR')
Dynamic Kinetic Resolution ('DKR')
Divergent Reactions of a Racemic Mixture ('DRRM')
Other Methods
STOICHIOMETRIC KINETIC RESOLUTION REACTIONS
Introduction
Kinetic Treatment
http://eu.wiley.com/WileyCDA/WileyTitle/productCd-3527330453.html
3-Chiral Separations: Methods and Protocols
https://books.google.ps/books?isbn=1592596487
Gerald Gübitz, Martin G. Schmid - 2004 - Science
Conventional methods for enantiomer separation on a preparative scale are fractionated ... It is not the aim of this book to give a comprehensive overview of all
https://books.google.ps/books?id=dmEyRNY-5owC&pg=PR5&lpg=PR5&dq=books+about+techniques+for+separating+enantiomers&source=bl&ots=Ly3ZabHYVT&sig=gQvmG0sfnSILRrIh5OtDCv2B5as&hl=en&sa=X&ved=0ahUKEwivm7ni1IHKAhWLvnIKHUGoDGgQ6AEILzAE#v=onepage&q=books%20about%20techniques%20for%20separating%20enantiomers&f=false
Hoping this will be helpful,
Rafik
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