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Questions related from Petru Lunca-Popa
Hello everyone 2-3 months I start getting weird XRD diffractograms. I was performing locked couple analysys on some polycrsitalline films. I am analysing those films for years so I know them quite...
21 February 2022 1,619 6 View
Hello I am measuring the reflectance of some coatings using a Perkin Elmer spectro (lamda 950). In order to increase the precision I bought (from PE also) a Al reference mirror. It cames with a CD...
09 January 2018 8,602 1 View
I am a very newbie in this Rietveld analysis. I am trying to fit my XRD pattern using (for a polycrystalline film) a CIF file. I know I am off stochiometry and I am sure my cell is deformed....
07 November 2016 4,609 7 View
I am having a Tauc plot showing two liniar segments. My question is related to the last liniar portion which is interesecting the x axis. I know the Band gap is obtained by extrapolating the last...
07 November 2015 3,847 12 View
Recently I switch on Brucker diffractometer (previously worked on Philips) and I am having a problem with alignment. It worked perfect until last week when something happened (possible...
01 October 2014 331 18 View
Trying to avoid the use of diborane as precursor for B I am looking for alternative precursors. Essays with Tri isopropyl, 3 etyl and tert buthyl Borate didnt give good results. Also the use of...
28 August 2014 1,341 5 View
For normal incidence of light can we really neglect the reflected light (in a spectrometer using an integrating sphere).
21 January 2014 1,445 6 View