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Questions related from Adam Baggott
If I have a Raman device that has a spectral resolution of 1 cm-1 then what is the uncertainty associated with my peak position measurements? For instance, if I measure my peak-fitted peak...
08 October 2018 2,607 4 View
I am trying to find out the ratio of alpha to beta grains in a bulk (non-powdered) sample of silicon nitride as well as their size distribution. What technique is best for determining this...
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I have read in the literature that secondary electrons (SEs) only escape from the top few nanometres (
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It is common practice to plasma etch a ceramic material in a barrel etcher in order to more clearly see the grain structure and intergranular phase. My question is, will the process change the...
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I am observing a ceramic under SEM and have noticed that in some stressed regions the signal appears to be brighter. Now I recognise that these brighter regions may just be due to charging but is...
06 September 2017 1,668 5 View
Hello there, So I have added a gold-conductive (via evaporation) layer to my bulk silicon nitride sample for use with SEM. Unfortunately the surface has become a bit dirty with dust and probably...
21 June 2017 8,398 3 View
Hi there, I am trying to use a Neon pen-ray source to calibrate my Raman spectra against thermal/instrumental fluctuations. I have placed the Ne source at various distances from my sample but am...
17 May 2017 1,300 0 View
Hi there, I'm using Raman spectroscopy to analyse the surface of my sample and need the laser spot size to be as small as possible. I'm using a 100x objective lens (the main determining factor of...
25 October 2016 1,875 1 View