The analysis of acetamiprid is approached in the scientific literature largely with liquid chromatography methods coupled to the different types of sensors but rarely in gas chromatography with an FID sensor. Are there any of you who have tried to do this type of assay, or those who can enlighten me on this methodological aspect? And why can't the FID sensor really detect this molecule despite the fact that it contains 10 carbon atoms?
So, here is the answer. However, low volatile compounds can also be effectively analyzed by GC. In case of Acetamiprid, you can find a very rich literature:
https://scholar.google.pl/scholar?q=acetamiprid+analysis+by+gas+chromatography&hl=pl&as_sdt=0&as_vis=1&oi=scholart
best regards,
GB
Simply derivatize the molecule for getting higher volatility thus getting analysis capability at GC systems, NPD could also be responsive since the molecule has nitrogens...tertiary amines could be the points that you may target to derivate the representative molecule for detection.
Check the link below as instructive;
http://old.iss.it/binary/moca/cont/Kataoka_1996.pdf