My sample is Ca2NaNb4O13 mixed with PEDOT:PSS and coated on ITO glass.

For CV measurement, I used 0.1 M Na2SO4 as electrolyte, Pt as counter electrode and Ag/AgCl as reference electrode.

For LSV measurement, I used 0.05 M KHCO3 as electrolyte and Pt as counter electrode.

Is there something wrong with my configuration?

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