Either elemental analysis or EDX analysis is better for identification low percentage nitrogen element. To me no need of quantitative accuracy also. Exact information on either present or not is required.
hi rajasekhar,
you must used a Kjeldahl method. you can search in the web
good luck
I would suggest ESCA so that you could get an in-depth analysis.
However if you would like to just prove the presence of nitrogen CHNS (elemental analysis) would do.
Hope this answers your question.
I agree with Dr. Kantheti. However you could also use EDAX to know the atmoic % of elements.
XRF is the best technique to analyze your sample
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