My friend and I have synthesized chalcone from 1-acetylnaphthalene and 2-fluorobenzaldehide, but the result was oil.
Do column purification
Check with TLC and purify with column.
I think ur compound maybe cummy oil. So monitor by TLC and do separation with column chromatography.
Follow the procedure of chalcone preparation
Equimolar concentration of acetophenone
(0.01 mol) and substituted benzaldehyde
(0.01 mol) was dissolved in 20 ml of ethanol.
To it, 15 ml freshly prepared 40%
sodium hydroxide solution was added (which
acts as catalyst).The reaction mixture was kept
undisturbed for 24 to 48 hours. The mixture was then
acidified with 1:1 hydrochloric acid and water.
Then it was filtered through vacuum, washed
with water, dried and recrystallized using
ethanol.
All the best
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