I am analyzing my sample for hydrogen evolution from acid halide in GC, but the oxygen peak is high how can I reduce oxygen peak in TCD.
What is your carrier gas in GC?
we use Ar as a carrier gas.
Do you see the nitrogen peak? Inject a small amount of air as a control for air leak into your system.
yes, nitrogen peak is also high.
Your oxygen peak is from air leaking into your system
thank you so much i will check by air injection .
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