As there are many procrdures...
1. KMNO4/KOH in water, T-->100 °C (laboratory)
2. Co(II) stearate/palmitate, H2O, O2/Air, T>50 °C (technology - !!reaction may be very exothermic!!)
Oxidize 2-methylpyridine (alpha picoline)to the corresponding acid in high yield you can use Alkaline KMnO4 or you can oxidize by coc. Nitric acid to give alpha picolinic acid.
I have made some carbon samples both CNTs and also activated carbons. How to we get clean SEM images. What is the sample preparation required? What is the sputtering time or cycles to be employed?
08 September 2018 1,461 5 View
Can litium which is very reactive be used as an reference electrode in an electrochemical process. If so how do we use it as a counter and reference electrode. Also handling this setup does it...
06 July 2016 7,128 2 View
I would like to monitor ester hydrolysis with GC. can any one help me by pointing out if there are any reactions that can be done so. Thank you.
06 July 2016 9,989 3 View
how do we coat activated carbon on to copper plate for studying its cpacitance? Are there any other methods?
02 March 2016 4,732 4 View
Can GCE be used with a oxidation potential of more than 3V?
09 October 2015 5,385 3 View
I am carrying out the oxidation of benzylic methyl group to carbonyls. I wanted to use SeO2 and so wanted to know how many mole equivalents of it is required to oxidise one mole of methyl group....
04 May 2015 2,351 5 View
What is fluorescent quantum yield and how do you calculate it? Are there many procedures and if there are which one is more accurate?
02 March 2015 4,887 10 View
Hello everyone, I recently submitted an article to Geotechnical Engineering (Proceedings of the ICE), and the current status has been listed as "EiC Pre-assessment: Ready" for the past 20 days. I...
10 August 2024 6,493 1 View
I'm cloning a fragment of 3200 nts into plasmid. The cloning was successful, however, 02 amino acids were mutated. Now I want to fix these 02 aa by site-directed mutagenesis technique using...
08 August 2024 4,645 2 View
Hello What should be done to separate and identify organic acids in HPC when their RetTime is the same?Like oxalic acid with Propanoic Acid.or acids that have a very close RetTime.
07 August 2024 8,782 3 View
Dear readers, Thanks for your attention. I am wondering about the health economic problem of quantifying the value of interventions which a) prevent, b) improve symptom profile and c) ultimately...
05 August 2024 3,246 1 View
I am performing ligation of the plasmid and a target gene. The steps I have taken are: 1. Double digestion of the plasmid and target gene 2. Ligation of the plasmid with the target gene 3....
05 August 2024 2,570 3 View
I am having an issue with my gel image where my PCR product is not appearing very bright on the gel. When I perform gel extraction, the A260/280 purity value is very low. I used the Qiagen gel...
05 August 2024 9,798 3 View
Hello. I am working on ROS production of two systems: system A is cerium oxide and hydrogen peroxide, system B is cerium oxide nanoparticle, hydrogen peroxide and potassium bromide. I did some...
04 August 2024 5,974 3 View
Why BaO (s) + H2O(l) ---> Ba 2+(aq) + 2 OH - (aq) if Oxygen loves owning all the electrons, why would it bind to hydrogen which competes with Oxygen for electron ownership more so than...
03 August 2024 5,392 1 View
I imagine the battery drives the graphite into a carbocation, then chloride is oxidized to donate the electron to the carbocation, but what pushes the lost electrons of chloride to be shared...
03 August 2024 5,384 0 View
How to calculate the molar proportions of the oxides from the XRF analyses?
02 August 2024 2,565 2 View