What is the best method for synthesising Dithiocarbazates (DTC) derivatives?

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Yasser Fakri Mustafa Popular answer

Dear Nabeel Arif Tawfeeq

I proposed that the discussion with Frank T. Edelmann is highly valuable.

Please review the article titled " Mild and efficient synthesis of carbazates and dithiocarbazates via a three-component coupling using Cs2CO3 and TBAI".

All the best

Frank T. Edelmann

Dear Nabeel Arif Tawfeeq, a very convenient solvent-free one-pot synthesis of dithiocarbazates is described in the attached article, which is Open Access. Good luck!

Dear Nabeel Arif Tawfeeq, did you try the synthesis and did it work?

Nabeel Arif Tawfeeq

Dear Frank T. Edelmann, Yes I did. I synthesised SBDTC & SMDTC but I'm looking for new method or odorless method if it is possible.

Dera Nabeel Arif Tawfeeq, thank you for the information. The two ligands (SBDTC & SMDTC) are described in the following articles. Both papers are available on RG. As you need the CS2 moiety in the molecule, I think there is no way to avoid working with carbon disulfide (under a well-ventilated fume hood). Thus I cannot really imagine an odorless method.

Article Hydrazine derivatives of the carbonic and thiocarbonic acids...

Article Metal complexes of sulphur and nitrogen-containing ligands: ...

Metal complexes of the two ligands have been reported in the articles cited below:

Article New metal complexes derived from S -benzyldithiocarbazate (S...

Article Synthesis, spectroscopic characterization and thermal behavi...

Thanks a lot Mr. Frank T. Edelmann.