Does it need acidic workup, or simple extraction with some organic solvent is OK. I already have this paper but some literature say we need acidic work up for complete removal of pthalylhydrazide (byproduct)
Final médium should be basic in order to allow extraction of the amine.
the reaction needs base as catalyst.
Good question
Regards
These article may help
https://onlinelibrary.wiley.com/doi/abs/10.1002/anie.196809191
DOI: 10.1055/s-1984-31028
The Gabriel synthesis of benzylamine: An undergraduate organic experiment
W. G. Nigh
I have to provide proof of submitted manuscripts especially those which are under review process.
06 July 2019 3,516 1 View
we want to protect one free -NH of piprazine with benzyl bromine using K2CO3 in CH3CN. any suggestion recommendation is appreciated.
03 April 2019 2,444 2 View
Mass analyzers in Mass Spectrometry
09 October 2018 4,245 3 View
is there any free software for this purpose, can we do it by Chemdraw.
06 July 2018 5,807 3 View
We need biochemist partners to perform MAO-B inhibitor or other enzyme inhibition activities on oue newly synthesized propargylamines.
31 December 2017 2,819 2 View
if possible please send me the pdf of book
31 December 2017 8,574 4 View
31 December 2015 7,792 15 View
Which one acts as more strong Lewis Acid?
08 September 2014 4,719 4 View
I made schiff base of carbazole aldehyde using excess of aniline, now I need to purify the product. I was just wondering will my schiff base remain stable at column and aniline will come first, or...
07 August 2014 1,298 8 View
My 1-bromomethylpyrene is pure by 1H, 13CNMR and GC-MS, but when ever I take Tlc it gives 4 or 5 spots. I am unable to understand. There is not a single extra peak in 1H and 13CNMR.
06 July 2013 5,589 2 View
How to calculate the RMSD values for a MD simulation using MOE?
07 August 2021 0 0 View
When I tried to energy minimization my system, I got fatal error as below. Fatal error: Atomtype opls_116 not found Although I've already added this line: ; include water #include "oplsaa.ff/spc.itp" to [molecultype] directive in my topology.
16 June 2021 0 0 View
effect of double bond on the flexibility of polymers
07 April 2021 0 0 View
I am writing to request some information for making polymer color flakes. I would appreciate the help.
17 March 2021 0 0 View
I'm involved in a study of odor control technologies for municipal wastewater treatment plant. One of the control options involves a chemical 2-stage (acid/alkaline) packed bed scrubber. The...
03 March 2021 3,661 2 View
I am at the beginner level in drug design and drug discovery, and I am interested to learn more about this field. Which books are highly recommended to start from and gives me all essential...
02 March 2021 8,437 2 View