I want to working on Fe/MgO compound by hydrothermal synthesis technique. Many research paper shows that it xrd pattern seems to MgO compounds but in my case i got Fe2MgO4 and Fe-Mg-O compound sot what should i need to do..?
I don't see the problem. You've probably excessively heated your system in air and formed a spinel. What do you want to do? Google "Ellingham diagram" and look at phase diagrams - I've done the latter for you...
Thank u sir Alan F Rawle for your nice explanation....Actually sir i want to synthesis Fe species content on MgO surface that seems to be a MgO structure by Hydrothermal treatment by using nitrate salt of both Fe and Mg at 180 C but most of the time i have seen that its form Fe2MgO4 and its different stoichiometric formation. Is it possible sir to synthesis Fe/MgO..