If we aim to have 80g of synthesized ZnO Nps using zinc acetate and sodium hydroxide what would be the measurements? and the process on doing it? Also what concentration should we use for it
During the synthesis of ZnO NPs via assisted microwave method (800kW, 5 mins), should we add all the NaOH solution (250mL, 0.5M) to the zinc acetate solution (250 mL, 0.2M) under constant...
13 November 2023 7,372 1 View
We synthesized ZnO NPs using Zinc Acetate and NaOH using a microwave (800W, 5mins). After some time, should the particles settle? How can be sure that it is in nanosize before we test it for TEM?
13 November 2023 3,283 7 View
We use Zinc Sulphate and Sodium hydroxide for the synthesis of ZnO NPs using chemical precipitation method. We mixed Zinc Sulphate solution and Sodium hydroxide solution (dropwise) at constant...
29 October 2023 2,475 1 View
We need to synthesize ZnO Nps using NaBH4 and Zn(NO₃)₂ how would it be done and what should we do to ensure a proper size in the ZnO Nps ?
25 September 2023 3,756 1 View
We are going to synthesize ZnO Nps using calamansi peel extract using NaBH4 and Zn(NO₃)₂ what would be the best way (we are thinking of chemical precipitation) to do it? also the amount needed to...
25 September 2023 2,027 0 View
We did macerate the grinded calamansi peels (127g) with ethanol (635 mL) for 36 hours then we are going to extract the calamansi peels via ethanol extraction using rotavap after it was...
25 September 2023 7,725 3 View
We are going to do a chemical synthesis of ZnO NPs using sodium borohydride and zinc nitrate after achieving the synthesis can we use a scientific oven since we don't have a calcifier to dry the...
01 January 1970 5,878 2 View
I have been using paraffin, but the deposited ZnO still detach from electrode. What is the best binder to modify graphite paste electrode with ZnO nanoparticles?
03 August 2024 4,624 3 View
Dear all, I have noticed, as the ZnO content increases, the Raman intensity at 100cm-1 also increases. However, there is a peak nearby at 130 cm-1, which I could not find in any paper related to...
28 July 2024 5,410 1 View
Hello everyone, A collaborator sent us his protocol in order to be able to use his immunohistochemistry kits. But one step contains PBS + 0.3% H2O2 + 0.1% sodium azide. Knowing the dangerousness...
23 July 2024 6,314 3 View
Recently I have submitted an article regarding MB dye degradation by ZnO nanoparticle. I received a suggestion to include the discussion on the effect of pH. I want to know what is the impact of...
19 July 2024 4,868 1 View
I need to make a stock solution for radioisotopic incubations of freshwater sediments to study dark primary productivity but I have some confusion as to how I calculate the concentration of 14C...
15 July 2024 5,898 0 View
I am working on powder metallurgy, and during the compaction process, the powder does not pelletize and remains in its powder form. To address this issue, I am considering using binders to improve...
13 July 2024 9,003 2 View
During the release test of Amphotericin B using 1% Tween 80, i observed three peaks even in the standard. The first peak consistently yielded results around 500%, while the other peaks showed...
08 July 2024 1,330 0 View
Hi, my research involves in ZnO synthesis. I have performed rietveld refinement of my samples and obtain a good fit using Fullprof suite software. However to obtain the crystallite size, the IRF...
07 July 2024 3,526 3 View
I did some column tests in my lab where I needed to detect the DOC fractions using LC-OCD. For the abiotic columns I used sodium azide to restrict the biofilm formation. I did LC-OCD to detect the...
07 July 2024 468 0 View
Hello All, I've been facing difficulty in executing geometry optimization of a sodium polyanionic phosphate (Na4Fe3P4O15) crystal in CASTEP (please find the input and output files attached). When...
07 July 2024 8,626 2 View