I want to quantify phenolics present in my aq. methanol extract using gc ms. But i want to make the extaract volatile so that it could separate out the phenolics. Please guide me to prepare my extract as such in easy way.
Thanks to all of you.After going through these articles i came to find out that most of have suggested to develop silyl derivative of phenolics. Now i want to know about the best method for silylation procedure.