How to differentiate between C13-NMR of bulk and porous g-C3N4 ?

01 January 1970 1 2K Report

I have prepared bulk g-C3N4 and with rope like crafted g-C3N4. I want to differentiate between their C13-NMR. Both are g-C3N4, but one is bulk and other with different morphology. I have confirmed their morphology with SEM, TEM and Also relaxed vibrations in FTIR spectra.

But I need experts opinions in this regard.

I will be thankful to all seniors and experts in this regard.

Muhammad Asim Khan

Naoropes or nanobelt crafted G-C3N4 has sharp and high intensity peaks. The analyzing 13C-NMR instrument is same and applied field is also same.

according to BET results, the surface area of Naoropes or nanobelt crafted G-C3N4 is also higher. Can we say the sharp peaks are due to nanoropes or nanobelts in the structure.

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Science method

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