We have single crystal instrument of agilent technologies supernova model with crysalis software. Initially we done powder XRD in same instrument it given good data with all peaks were detected but it has lack of baseline. Let me know how to correct the baseline in this software. Help me please. The XRD graph is attached here.
thanks in advace
check the linke below
http://www.clays.org/journal/archive/volume%2049/49-5-398.pdf
I am sure that baseline correction feature will be there in your XRD software. If not, then you can use Origin software and use baseline correction option given by clicking first analysis option and then spectroscopy, where you will find option create baseline. Other XRD softwares such as High Score plus also have baseline correction option. If you are unable to do that then send me your data in .txt file. I can do it for you.
Thank You very much Kapil Sood, I have done baseline correction using Origin software. but i think data generated after baseline correction is not good for publication . i would like cross check the baseline correction with you so i will send you data file if provide ur mail id. or send a text mail to me on [email protected]
It looks like you are getting a lot of air scattering at low angles, and seeing the direct beam through the beamstop. Have you tried to adjust the beamstop to remove this? It will make analysis much easier as well as increasing your signal to noise.
You can use baseline correction feature in Origin software. See it here: http://bit.ly/2tvAskQ
Please see this video
How to Correct Baseline in Origin
https://www.youtube.com/watch?v=sUi_0jWKDWs
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