Thank you for showing your interest here. For research I recently purchased 3 different nano-particles online, but when I received the particles, they were tagged with name of some other material. On asking the supplier about the issue, they told us that the courier service has licence to deliver some specific material so they removed the actual tag and placed new tags. Since we are not satisfied with their response as they did not tell this to us at any point of delivery, so we have filed dispute with the supplier. Now we want to identify the particles so that we can use them in our research. We have performed the XRD test and have created the graphs in OriginPro. We could have done it ourselves but since we have never done it before so we require an expert to just confirm from the graphs that they are the actual particles we ordered so that we can use them in research. Later we will do the complete analysis ourselves, we request anyone to just confirm if we have received the correct particles or not so that we can take action on the order dispute. We will be really thankful if anyone can help us in this regard. Thank you so much for your time.
Regards,
Muhammad Muzammil Azad
This article may help you
Article Determination of nanoparticle sizes by X-ray diffraction
The correct method to determine the crystallite size is by Williamson and Hall.
Basheer AL-Anesi thank you for your reply it is helpful, but the main issue is the identification of nano-particle material. Is there some way we can identify the material of nano-particles from the XRD test data. Your help in this regard will be highly appreciated. Thank you
Anup Debnath thank you for your reply it is helpful, but the main issue is the identification of nano-particle material. Is there some way we can identify the material of nano-particles from the XRD test data. Your help in this regard will be highly appreciated. Thank you
If you can mentione the names of three materials here that may let us to help.
I suggest you to use EDS technique that maybe help you.
Basheer AL-Anesi we have 3 materials
1. Silicon dioxide
2. Zirconium hydroxide
3. Aluminium hydroxide
We also have their XRD data.
Anup Debnath I will contact you personally after you get free on 27th January. Thank you so much for showing your interest.
Anup Debnath I have left you a personal message regarding the issue I am facing. Thank you so much for your help.
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- Methodology
- Crystallography
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